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1 article(s) from Kraus, Alexander

One-pot syntheses of blue-luminescent 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones by T3P^® activation of 3-arylpropiolic acids

Melanie Denißen,
Alexander Kraus,
Guido J. Reiss and
Thomas J. J. Müller

Beilstein J. Org. Chem. 2017, 13, 2340–2351, doi:10.3762/bjoc.13.231

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Scheme 1: Mechanistic rationale and optimization of the domino synthesis of 4-arylnaphtho[2,3-c]furan-1,3-dio...

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Scheme 2: Domino synthesis of 4-arylnaphtho[2,3-c]furan-1,3-diones 2 via in situ activation of arylpropiolic ...

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Scheme 3: Optimization of the synthesis of 2,4-diphenyl-1H-benzo[f]isoindole-1,3(2H)-dione (4a) by imidation ...

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Scheme 4: Pseudo three-component synthesis of 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones 4.

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Scheme 5: Modified sequence for the synthesis of acceptor-substituted 4-aryl-1H-benzo[f]isoindole-1,3(2H)-dio...

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Figure 1: The ORTEP-style plot of crystal structure 4b (ellipsoids are draw at the 40% probability level).

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Scheme 6: Pseudo four-component synthesis of (E)-2,9-diphenyl-3-(phenylimino)-2,3-dihydro-1H-benzo[f]isoindol...

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Scheme 7: Synthesis of 6-phenyl-12H-benzo[f]benzo[4,5]imidazo[2,1-a]isoindol-12-one (6).

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Figure 2: The ORTEP-type plot of the crystal structure 5 (left) and a centrosymmetric dimer formation by π–π ...

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Figure 3: The ORTEP-type plot of the asymmetric unit of the crystal structure 6 (top) and π-stacking interact...

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Figure 4: Emission properties of compounds 4a,b,d–f, 5, and 6 under handheld UV-lamp (λ_exc ≈ 350 nm).

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Figure 5: Relative emission intensities of compounds 4a,b,d–f (recorded in CH₂Cl₂ UVASOL^® at T = 293 K; λ_exc ...

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Figure 6: Absorption and emission properties of selected imides 4 measured in CH₂Cl₂ UVASOL^® at 293 K with λ_e...

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Figure 7: Hammett–Taft correlations of the emission maxima (red circles, l_max,em = 4274 · s_R + 24495 [cm⁻¹], R...

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Figure 8: Relative emission intensities of the 1-phenyl-2,3-naphthaleneimide 4a (blue) and the pentacyclus 6 ...

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Published 03 Nov 2017

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One-pot syntheses of blue-luminescent 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones by T3P® activation of 3-arylpropiolic acids

One-pot syntheses of blue-luminescent 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones by T3P^® activation of 3-arylpropiolic acids